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Pictures from an organic chemistry laboratory
The source of your daily dose of applied organic chemistry in pictures, directly from an organic chemistry laboratory.
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All images posted here are licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License: ... Follow @labphotographer
Have You seen my portfolio? It’s over here!
Bored? Click here to see a random post from the blog!
Buy the best pictures from the blog at society6!
If You could contribute this project, I would be really thankful:
Crystals of a partially crystallized acid chloride derivative. For a week, it was a clear liquid with a horrible odor, but after the weekend these nice crystals formed at the bottom of the flask.
No one ever described this compound previously, so there is no reference for it, that should it be a solid or a liquid.
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The plan was to grow a single crystal from this compound for a single crystal X-ray crystallographic analysis to know the exact structure of the compound. But sadly it only gave these fluffy needle like crystals from every solvent what could be used for it’s crystallization.
Good point: it looks great on a photograph(:
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Sublimed, superpure crystals of trichloromethyl-trimethylsilane at the wall of a flask.
Interesting about this compound, besides it costs much if you would like to buy it, that it has a melting point at 130 °C if it’s sealed, but if you heat it in an open flask, it will sublime away in no time. And it has a quite characteristic odor, similar to camphor.
Both picture is part of my portfolio, what is the collection of the best pictures from the blog. It could be purchased at Society6 as a high quality great looking print now with a FREE Worldwide Shipping til’
October 11, 2015 at Midnight Pacific Time. To get a picture on your wall, just visit this link: https://society6.com/labphoto?promo=NJYKQ8VB9QKT
Another snapshot from the still pot.
The greenish crystalline compound is a decomposition product of the ferrocene where the iron in in +2 oxidation state. The black is some polymerized tarry byproduct that formed from the decomposition of 1,1′-diacetylferrocene.
However, it looks great and its part of my portfolio, what is the collection of the best pictures from the blog. It could be purchased at Society6 as a high quality great looking print now with a FREE Worldwide Shipping til’ September 13, 2015 at Midnight Pacific Time. To get a picture on your wall, just visit this link: https://society6.com/labphoto?promo=NJYKQ8VB9QKT
Beautiful crystals of a sublimed perfluoroalkyl-thioamide. A hard to prepare, but currently completely useless compound what was isolated as a byproduct of a reaction.
Good point: it looks great!
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There are always random flasks in the lab. This contained some BINOL (1,1’-Bi-2-naphthol) what didn’t reacted as we wanted, so if was left under the fume hood to crystallize. After a week I found these little crystals at the bottom of the flask(:
The best pictures from the blog, what are tagged as my portfolio, including these pictures, could be purchased at Society6 as a high quality great looking print now with a FREE Worldwide Shipping til’ April 12, 2015 at Midnight Pacific Time. To get a picture on your wall, just visit this link: http://society6.com/labphoto/prints?promo=NJYKQ8VB9QKT
Crystals of sublimed 2-(trifluoroacetyl)pyrrole.
The raw reaction product what was an off-white crystalline compound with a melting point 50 °C was loaded in a test tube and left there for a few months. For now, these crystals formed at the wall what are perfectly pure 2-(trifluoroacetyl)pyrrole.
If this compound is left on a Petri dish for a day, most of it will sublime away.
My new favorite: fluorescent crystals at the side of a test tube.
Something new was made what crystallized on standing. Previously I could only make this compound as a powder and I was unable to grow crystals from it, since it’s nearly insoluble in everything, but now, with a little trick these nice crystals formed what are highly fluorescent and look great.
The bottom picture is cropped from the upper photo.
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Found an ampule under a fume hood with thiophosgene written on it. Probably mainly thiophosgene was in it long ago, since thiophosgene is a red liquid and not an adorable looking colorless crystalline solid.
Thiophosgene is similar to phosgene (COCl2), the only difference that a sulfur is on the molecule instead of the oxygen, so it could be written as CSCl2. It is a red liquid with probably a horrible odor, but since it’s highly toxic it’s not recommended to sniff it.
The best pictures from the blog, what are tagged as my portfolio, including these pictures, could be purchased at Society6 as a high quality print: http://society6.com/labphoto.